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MgO-C的氧化-还原反应在镁砂-石墨复合材料中的作用
作者:林育炼 Charles.E.Semler 
单位:冶金鄗洛阳耐火材料研究所  美国俄亥俄州立大学陶瓷工程系 
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出版年,卷(期):页码:1987,15(4):364-371
DOI:
摘要:
研究了海水镁砂-石墨复合材料中涉及氧化-还原反应的显微结构的作用。选择粒度不同的粗颗粒、中间颗粒和细颗粒试样在1600℃下煅烧不同时间。对煅烧后的试样的氧化百分率、失重、致密层和致密层的显微结构特点作了鉴定。观察到材料和煅烧条件不同的试样的逐渐鼓胀过程,并对此现象作了解释。讨论了致密层形成机理和速度。着重考虑了粒度对控制脱硬的作用。
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The microstructural effects associated with oxidation-reduction reaction in seawater magnesia-graphite composite material have been studied. Samples of coarse, intermediate and fine particle size were fired at 1600℃ for various periods. Evaluation of the fired samples for oxidation percentage, weight loss, dense zone and microstructural characteristics of the zone is carried out. Gradual swelling of samples observed in different firing conditions is illustrated. Formation mechanism of the dense zone and the rate of formation are discussed. Emphasis is put on the effect of particle size on the control of decarbonization.
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参考文献:
[1] G.D.Pickering and J.D.Batchelor, Amer. Ceram. Soc. Bull., 50[7] (1971) 611. [2] R.J.Leonard and R.H.Herron, J.Amer.Ceram.Soc., 55[1] (1972) 1. [3] B.Brezny and R.A.Landy, Trans.J. Brit.Ceram.Soc., 71[6] (1972) 163. [4] S.C.Carniglia, Amer.Ceram.Soc.Bull., 52[2] (1973) 160. [5] B.H.Baker, B.Brezny, and R.L.Shultz, Amer.Ceram.Soc.Bull., 54[7] (1975) 665. [6] ibid., 55[7] (1976) 649. [7] S.M.Kim, P.S.Nicholson, and W.K.Lu, Amer.Ceram.Soc.Bull., 57[7] (1978) 649. [8] H.M.Mikami and J.R.Martinet, Refr.J.[6] (1980) 25. [9] B.Jackson and R.Webster, Iron and Steel Intern.April(1980) 67. [10] A.Watanabe, H.Takahashi, T.Matsuki, et al.,Preprint of lst Intern.Conf.on Refr., Tokyo, Japan(1983) 125. [11] R.Brezny and C.E.Semler, J.Amer.Ceram.Soc., 67[7] (1984) 480. [12] M.Ikeda, Nippon Steel Corp., Personal Communication, Himeji, Japan, Nov.(1983) .
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